GCMS results for sample AE00467, Jan 24 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00467.D Vial: 7 Acq On : 11 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 8 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 25.67 0.18 ug/L 109244 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 83 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 56 3 2-Norbornanone, 1-(epithioethyl)... 228 C11H1603S 001782-93-0 36 4 (!R,3aS,7aS)-7a-Hydroxyethyl-l,4... 224 C14H2402 128790-34-1 10 Abundance Scan 1953 (25.671 min): 00467.D (-) m/z 64.00 100.00% 64

5000 192

96 128 160 . 224 256 25.40 25.60 25.80 26.00 Of 40 ' 1 I... , 76 . 1 ■ ■ i ' ' ll, I,...... I*__ I,.. m/z 191.80 49.42% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195809: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64

5000 TIP 192 25.40 25.60 25.80 26.00 96 128 160 m/z 127.90 22.09% 0 48 ■ ’ । ■ i ■ ■ i 180 . ... .. . 1 1 1 1 1 i 1 । 1 1 i ' 224 1 1 । > • । 1 । I '1 | 256 । । • 1 1*। । । n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195803: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 6l4 TIT 25.40 25.60 25.80 26.00 5000 m/z 159.90 21.52%

J 256 128 160 96 192

n/z-> 0 44 • ■ 11 • ■ > । 40 60 — .. 80 I- .. 1 A 224 100 120 140 160 180 200 220 240 260 ■ ।1 ■ ■ ■ । '

Abundance #156398: 2-Norbornanone, 1-(epithioethyl)-7,7-dimethyl-, S... r 64 120 25.40 25.60 25.80 26.00 93 m/z 95.90 18.73% 5000 107 53 164 79 151 34 0 ■ > i ■ ' ' I ‘‘I* ■ ■ i ■ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 25.40 25.60 25.80 26.00

00467.D SCAN508.M Mon Jan 14 10:47:07 2002 Page 10

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