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GCMS results for sample AE00467, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051453–000051470

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051463
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Llbrary Search Compound Keporc

Data File : C:\MSDCHEM\1\5973N\O2 JAN11\OO467.D Vial: 7 Acq On : 11 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 PERDEUTEROCYCLOHEXANE $$ Cy... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.84 1.60 ug/L 971842 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 PERDEUTEROCYCLOHEXANE $$ Cyclohe... 96 C6D12 001735-17-7 40 6 2 2-Norbornanone, 1-(epithioethyl)... 228 C11H1603S 001782-93-0 28 w8r, 3 PERDEUTEROCYCLOHEXANE 96 C6D12 001735-17-7 7 So* 4 Cyclohexane-dl2 96 C6D12 001735-17-7 7 Abundance Scan 1705 (22.840 min): 00467.D (-) m/z 63.95 100.00%

A 64 160

96 224 5000

.128 192 n/z-> 20 Oh 44 • i > ■ > ■ । I 40 60 80 - 100 120 140 .160p.180... . 200 220 22.60 22.80 23.00 23.20 m/Z 159.90 96.51% Abundance #3552: PERDEUTEROCYCLOHEXANE $$ Cyclohexane-d12 64 46 96 5000 ■ i ■ ■

78 22.60 22.80 23.00 23.20 30 m/z 95.90 51.31% Oh I ' ' I ' ■ I "1 • 1 i ' n/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #156398: 2-Norbornanone, 1-(epithioethyl)-7,7-dimethyl-, S... 64 93 120 10 22.60 22.80 23.00 23.20 5000 107 m/z 223.80 47.70% 53 164 79 151 34 Oh ' 1 I ' T • i n/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #3551: PERDEUTEROCYCLOHEXANE ■ ' i ' *f 1 15 64 22.60 22.80 23.00 23.20 96 m/z 161.90 18.94% 46 5000

30 78

oh 1 • ■ i • — ‘ I’’ n/z-> 20 40 60 80 100 120 140 160 180 200 220 22.60 22.80 23.00 23.20

00467.D SCAN508.M Mon Jan 14 10:47:07 2002 Page 7

NYC-WTC_000051463

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NYC-WTC_000051463Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗

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