NYC-WTC_000051453
Laboratory report showing GCMS analysis of sample AE00467 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 18 pages
GCMS analysis results for sample AE00473, Jan 18 2002
Machine-extracted title · confidence 100%Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00473 conducted on January 18, 2002.
NYC-WTC_000051283–000051300Folder label: “GCMS X 1/8/02 A 1/10/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00466.D Vial: 4 Acq On 10 Jan 2002 5 :18 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 2-Norbornanone, 1-(epithioe... Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T. 22.83 4.20 ug/L 2434750 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Norbornanone, 1-(epithioethyl)... 228 C11H1603S 001782-93-0 28 2 (1R*,4R*,5S*)-1-CARBETHOXY-4-MET. .. 234 C15H2202 043219-76-7 9 3 Cyclohexane-dl2 96 C6D12 001735-17-7 7 4 Ethane, chloro- (CAS) $$ Chloroe... 64 C2H5C1 000075-00-3 5 Abundance Scan 1704 (22.828 min): 00466.D (-) m/z 64.00 100.00% 64 160
5000 96 224
128 । 192 22.40 22.60 22.80 23.00 23.20 oh 36 ■ ' i ■ ■ 1 ' t | 76 ' ■ ■ । > l..... .1°...... .. 256 m/z 159.90 74.81% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #156398:2-Norbornanone, 1-(epithioethyl)-7,7-dimethyl-, S... 64 120 93
5000- 107 i ' ' 1 1 i 1 ' 1 ' i ' ' ' ' k1 1 ' i 1 ' 1 53 164 22.40 22.60 22.80 23.00 23.20 79 151 m/ Z 95.90 40.03% 34 | Oh 11 1 1 ' ■ I TTTT TT 1 ■ i ■ ■ ■ ■ 1 1 1 1 1 i ' 1 1 1 I ' ' ■ ■ i ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #165203: (1R*,4R*,5S*)-1-CARBETHOXY-4-METHYL-8-METHYLENE-S... 160 91 119 9 105 22.40 22.60 22.80 23.00 23.20 5000 m/z 223.80 39.87% 188 234
oh m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #3553: Cyclohexane-d12 T111r 46 64 22.40 22.60 22.80 23.00 23.20 m/z 161.90 16.25% 96 5000 30 78
n/z-> Oh 20 1 44 ■ 'T' 40 60 1 1 i 1 ■ 80 100 120 140 160 180 200 220 240 260 22.40 22.60 22.80 23.00 23.20
00466.D SCAN508.M Fri Jan 11 10:08:36 2002 Page 8
NYC-WTC_000051294
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NYC-WTC_000051294Source: NYC Law Department, mirrored locally
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