GCMS analysis results for sample AD31676, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data.File : C:\MSDCHEM\1\5973N\O2JAN23\31676.D Vial: 1 Acq On : 23 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Norbornanone, 1-(epithioe... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.85 4.34 ug/L 2444020 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Norbornanone, 1-(epithioethyl) .. . 228 C11H1603S 001782-93-0 28 2 1,2,5,6-tetrathia-3,7-dimethyl-c... 212 C6H12S4 116664-31-4 7 3 Cyclohexane-dl2 96 C6D12 001735-17-7 7 4 PERDEUTEROCYCLOHEXANE $$ Cyclohe... 96 C6D12 001735-17-7 5 Abundance Scan 1706 (22.851 min): 31676.D (-) m/z 64.00 100.00% 64 160

5000 96 224 ■1 ■ • । ■ ■ ■ ■ । ■ ■ ■ ■ । ■11 * ■ • 128 192 22.60 22.80 23.00 23.20

nz-> 0b 20 **1*1 44 40 60 17680— 100 120 - 140 160 180 200 220 L m/z 159.90 81.80%

Abundance #156398:2-Norbornanone, 1-(epithioethy!)-7,7-dimethyl-, S... 64 93 120

5000 107 T TI——TTTT 53 79 164 22.60 22.80 23.00 23.20 151 m/z 95.90 43.30% 34 I I

A 0b ■ ■ i • ■ • i 1** • • i ' 1 ' i ' 1 r ■ i ■ ■ ■ • i ‘ • m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #132056: 1,2,5,6-tetrathia-3,7-dimethyl-cyclooctane $$ 1,2... 41 1 1 i 1 ■ ■ ■ i T 73 138 22.60 22.80 23.00 23.20 212 m/z 223.80 39.63% 5000 106

miz-> 20 ob Abundance ■ ■ i 1 1 ■ ■ i 40

46 60 64 ■ ■ i ■ ■ • 1 i ■ ■ ■ ■ i ‘ 1 ■ • i ■ ■ ■ ■ i ■ ' ■ ■ i ' ‘ ■ ■ i ‘ 1 80 100 120 140 160 #3553: Cyclohexane-d12 180 200 ————— 220 A. 22.60 22.80 23.00 23.20 m/z 161.90 18.25%

A. 96 5000 30 78

miz—> ob 20 L40 4460 ** i ■ ■ • । 80 • 100 120 140 160 180 200 220 22.60 22.80 23.00 23.20

31676.D SCAN508.M Thu Jan 24 09:57:33 2002 Page 9

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