GCMS analysis results for sample AE00838, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00838 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050411–000050420

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN23\00838 . D Vial: 7 Acq On : 23 Jan 2002 7:54 pm Operator: Sample : 508 scan Inst : Instrumen Mise . : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* .Peak Number 3 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 88331 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 78 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 3 1-amino-2-methyl -4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 50 Abundance Scan 1656 (22.280 min): 00838. D (-) m/z 192.10 100.00% 1912

5000

82 96 146 160 - ajannips 22.00 22.20 22.40 22.60

n/z—> 0’ 42 mmmmmmmmmmmpmp 66 I I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 2(» I m/z 191.10 17.79% Abundance #102588:4-METHOXY-.BETA-METHYLCINNAM1C ACID $$ 2-Butenoi... 192

108 5000- — ————— 22.00 22.20 22.40 22.60 146 175 m/z 146.10 16.34% fl 0- ■■■i•■ “ i■'■•i “ ■'i■■■■ i “ i'" ■ i “ “ i11' 11.. 11. >.. 11 >.. ।.. ■ i ■ ■" i ■ ‘" i ■ hiyairr Tmn iz--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 A ■ ■ ■ i ■ ■ ■ 1 i r / ' i ■ ■ ■ ‘ i ■ ■ ■ ■ 22.00 22.20 22.40 22.60 5000 82 m/z 96.10 14.32% 54 110 30 94 160 iz-> 0 h -HP 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m 111n Abundance #101918:1 -amino-2-methyl-4-isopropyI-thiotriazaphospholin... II > ■ i ■ ■ ■ • i ■ 159 19 2 22.00 22.20 22.40 22.60 m/z 193.10 13.55% 5000-

144 177

m/z—> 0 *’’I’’4***’t’4*d*****/t1****H***11****1**+1****1****H* 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 2(X) । ■ 1111 111111 r 11111 m **1/41111*4*1)1 22.00 22.20 22.40 22.60

00838.D SCAN508.M Thu Jan 24 09:57:26 2002 Page 5

NYC-WTC_000050418

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NYC-WTC_000050418Source: NYC Law Department, mirrored locally

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