GCMS analysis results for sample AD28861, Dec 17 2001

NYC 9/11 Public Portal Document Library Search Compound Report • Data File : C:\MSDCHEM\l\5973N\02FEB01\28860.D Vial: 3 Acq On : 1 Feb 2002 12:14 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 2-Norbornanone, 1-(epithioe... Concentration Rank 5 R.T. EstCono Area Relative to ISTD R.T. 23.68 0.23 ug/L 168363 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------- 30 1 2-Norbornanone, 1-(epithioethyl)... 228 C11H1603S 001782-93-0 33 • 2 N-Methyl-l,2,4-dithiazolidine-3,... 149 C3H3NO2S2 018137-43-4 9 3 8-Oxo-8H-indeno[1,2-d]-1,2,3-thi... 188 C9H4N20S 000000-00-0 4 4 Sulfur dioxide $$ Fermenicide po... 64 02S 007446-09-5 4 Abundance Scan 1779 (23.684 min): 28860.D (-) m/z . 64.00 100.00% 64 160 5000 149 96 224 192 23.40 23.60 23.80 24.00 43 128

miz-> 0: 484.it .. •■i••■•i •■ •■i I nyr i ■• • • i ■ “ ‘ r “11 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 ‘ • i ■" • i ‘1 ■ ■ ‘I’T m/z 159.90 67.86% Abundance #156398:2-Norbornanone, 1-(epithicethyl)-7,7-dimethyl-, S... 64 93 120 J/A 50001 107 53 164 23.40 23.60 23.80 24.00 79 151 m/z 149.10 46.31% 34 O ■'i ""111' — "10199131101111133111893 ’I’*’I’———94’4tH**81’*4*184 iz-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #44890: N-Methyl-1,2,4-dithiazolidine-3,5-dione $$ 1,2,4-D... 64 T T I ' ' ' ' I ' ‘ 23.40 23.60 23.80 24.00 5000 149 m/z 95.90 36.18%

m/z-> 01

Abundance ।।... t.... । 1[l 111 • 1111 h1]।।t....t।j.... j.. 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 #97239:8-Oxo-8H-indeno[1,2-d]-1,2,3-thiadiazole 121

„/W/ 132 KO 23.40 23.60 23.‘80 24.00 m/z 223.80 30.83% 5000

0 1.| 93

| .... । .... । .... । .... । ,■> I I H I 11 1 1 I j ■ 11 1 | 188 kmmmmHTTT „/uMuu iz-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 23.40 23.60 23.80 24.00

28860.D SCAN508.M Mon Feb 04 08:41:06 2002 Page 12

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