GCMS analysis report for sample AE01511, March 2002

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GCMS laboratory results for sample AE01511 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010047–000010065

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB21\01511.D vial: 2 Acq On : 21 Feb 2002 4:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.11 ug/L 73848 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole. .. 192 C13H8N2 057102-93-9 72 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 64 3 Benzo[1,2-c:3,4-c]bis(isothiazol ... 192 C8H4N2S2 074960-05-7 64 4 2,4-Diamino-6-(hydroxymethyl )pte... 192 C7H8N60 000945-24-4 50 Abundance Scan 1675 (22.283 min): 01511 .D (-) m/z 192.00 100.00% 192

5000 ................ . 96 146

miz-> O' 70 82 , i ■ “ ' i ■ • “ i • • ■' i " ■ ■ 11 ■ “ i'' • ■ i'' ■ i • ■ ■ ‘1’11110171111/1163

30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TI8 4ll m/z 22.00 22.20 22.40 22.60 95.90 16.98% Abundance #103424:3-Cyanocarbazole $$ 9H-CarbazoIe-3-carbonitrite (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 146.10 16.88%

n/z-> 0 . ■ । >... ।.... ।.... ।.... ।.. ■. ।> t.. mmm 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ‘!4* 138 l Abundance #102010:2,4-Diamino-6-(hydroxymethyl)pteridine 192 163 . .... N... / ) 22.00 22.20 22.40 22.60 5000 m/z 193.00 13.95% 66 .. 121 125 146 34 01 .j(j.. ■ । .................1.12 .....1L “ ।1 “ ■।1 ■1 ■ ।'" ‘ । ■ ■ ■ ■ । “ > ■ । ■■ । ■1 11 > ■ ■1111 “ n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102104: Benzo[1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... 192 22.00 22.20 22.40 22.60 m/z 191.00 12.04% 5000 45 148 57 69 82 96 121

miz-> 0 .......... ..... 1...... 1 | "I0000—000Tpand 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 .. X.....'In.. T T 22.00 22.20 22.40 22.60

01511.D HP022102.M Mon Feb 25 10:55:18 2002 Page 12

NYC-WTC_000010062

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GCMS analysis report for sample AE01547, March 2002 · Box DEP Box 14

NYC-WTC_000010066

GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

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