DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02386.D Vial: 2 Acq On : 27 Feb 2002 4:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 11 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 127217 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 59 3 Benzo[1,2-c:3,4-c]bis(isothiazol... 192 C8H4N2S2 074960-05-7 59 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 53 Abundance Scan 1675 (22.283 min): 02386. D (-) m/z 192.00 100.00% 192

5000

92 96 ' I ' ' ' ' I 1 1 22.00 22.20 22.40 22.60 42 118 70111111I11111.11111 .......... 146 160 II m/z 96.00 0- THTT 11111111 I"' ----- I’’ 14.72% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 164 m/ z 14 6.0 0 12.66% 96 138 0 i | । i i i | i । । i | i । i । | । । । । | i । । । [ i : i i | i 1.......... 1 1'1 '''I Il, '' 11 1 11 '' I'' m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103959: fluorene-9-spiro-cyclopropane 192 1....... {Ns 165 22.00 22.20 22.40 22.60 5000 m/Z 193.10 12.12%

m/z-> .40........... 0- i । । ■ । । । । । 87.8.......... ............ TPH 4 i i । j । i i i । i i rl [ i 1ror11m7 11 1 1 | 1 11 1 1 1 11 1 1 ' 1 1 1 1 11* i [ i i । 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102104: Benzo[1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... / 1 / 1 192 22.00 22.20 22.40 22.60 m/z 191.00 11.85%

5000 45 148 57 69 82 96 121 0 n | ........... ....... 1 ,,, I.................. I.................. I'11 ‘ I' ■ ‘ ‘ 111111'11111111111 ......... I n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

32386.D HP022102.M Thu Feb 28 08:47:10 2002 Page 13

NYC-WTC_000005042

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999