DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02090.D Vial: 7 Acq On : 26 Feb 2002 7:45 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Phenanthrene, 9-methyl- $$ ... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 100190 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 2 Benzo[l,2-c:3,4-c]bis(isothiazol... 192 C8H4N2S2 074960-05-7 59 3 2-CYANOCARBAZOLE $$ 9H-Carbazole ... 192 C13H8N2 057955-18-7 50 4 3-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 057102-93-9 50 Abundance Scan 1675 (22.283 min): 02090.D (-) m/z 192.00 100.00% 192

5000

1 r i ■ 1 ■ ■ i ■ ■ 62 96 0 42 —Pmmmm 70 82 | 120 -H 146 160 .... II,, lrrian TIE 22.00 22.20 22.40 22.60 m/z 146.10 14.69% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

5000 *m 22.00 22.20 22.40 22.60 m/z 96.00 12.81% 96 165 88 1 139 152 1 176 0 '111" ' I ■ " ■ i " '' i " 1111" 11'11' i " ■' i1" 111" ... ........... 11'' >-f t < ।' 1111111111 i't /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102104: Benzo[1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... 192

22.00 22.20 22.40 22.60 5000 m/z 191.00 11.97% 45 148 57 69 82 96 121 165 li --- - Of m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 22.00 22.20 22.40 22.60 m/z 193.10 11.75%

5000

os 164 0 ■' I' ■1 ■ I • " ■ I ‘11' I ■ ■1 ■ 11" ■ 1111'' I" ■' 111111"111"138 II 11' " l r'111 1 ''I'' " 11' " I'''' yp-T m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02090.D HP022102.M Wed Feb 27 08:35:28 2002 Page 12

NYC-WTC_000004680

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999