GCMS analysis report for sample AE01511, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

’ Data File : C:\MSDCHEM\l\5973N\02FEB21\01511 .D Vial: 2 Acq On : 21 Feb 2002 4:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 3,6-Dimethyl-triazolo(4,3-b... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

24.86 0.04 ug/L 26864 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dimethyl-triazolo(4,3-b) (1,2.. . 149 C6H7N5 000000-00-0 5 2 3,6-DIMETHYL-TRIAZOLO[4,3-B]-1,2... 149 C6H7N5 061139-71-7 5 3 2-Ethoxy-1-(3'-pyridyl)ethylene 149 C9H11NO 000000-00-0 4 4 2-(2-Carboxyvinyl)pyridine, tran... 149 C8H7NO2 007340-22-9 4 Abundance Scan 1903 (24.857 min): 01511.D (-) m/z 149.00 100.00% 149

5000

41 24.60 24.80 25.00 25.20 01- m/z 41.10 13.08% nz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44984:3,6-Dimethyl-triazolo(4,3-b)(1,2,4)-triazine 149

5000 81 24.60 24.80 25.00 25.20 53 m/z 150.00 11.47% 41 121 0-TPTTTT ■ • । ■ i ■1 • • i ■ ■ ■ • i1' •111 ■ ■ • i ■ ■ ■11 ■ • ■ ■ i ■ ■ niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44967:3,6-DlMETHYL-TRlAZOLO[4,3-B]-1,2,4-TRlAZINE $$ 1,2... 149 ■ ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ' 24.60 24.80 25.00 25.20 5000 81 m/z44.00 8.45%

41 53 121 0 11'11' 1'1 • i • • • • i > ■ ■ • i11 ■ ■ I ■ ■ ■ ■ i ■ ‘1 ■ i1 ■'' i ■ ‘ ' i' ‘ ’11 tJz~> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #45160:2-Ethoxy-1-(3’-pyridyl)ethylene

92 121 149 24.60 24.80 25.00 25.20 5000 65 39 29

0 ■ i1 ■ ■ ‘ i uam 111111111.'11111'11 ■ i ■ ‘ ■ ■ i ■' • • l ■ ■ ■ ■ i n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150

01511.D HP022102.M Mon Feb 25 10:55:18 2002 Page 13

NYC-WTC_000010063