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GCMS blank analysis results for sample AE00027, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.

NYC-WTC_000050716–000050734

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050731
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02JAN25\0104BA.D Vial: 1 . Acq On : 25 Jan 2002 10:12 am Operator: Sample : lab blank 1/4 a Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 2-CYANOCARBAZOLE $$ 9H-Carb... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 104829 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 2 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 3 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 Abundance Scan 1656 (22.280 min): 0104BA.D (-) m/z 192.10 100.00% 1912

5000 .............. 82 70 11...,.ll. I■■ 96 120 146 160 22.00 22.20 22.40 22.60 44 "I1 "'I''"1"" 111 li । rm |. । u 111 > | +m m/z96.00 15.98% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420:2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 m/z 193.10 14.68% 06 164 TT TTrr TOTTDTTTmun I 138 II 111" n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 22.00 22.20 22.40 22.60 5000 m/ Z 146.10 14.32% 146 175

■111 M11u 111'11111H ■ i ■" ■ i ■ ■ " r ■ I ■ ' " | ' I u | • " I | I I ' I " " 111" 11 1TTT TTrur mfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 22.00 22.20 22.40 22.60 m/z 191.10 13.79% 5000

96 164 | 138 TTTTTTTTTTTTTTTTTTTTTT I............ H I ‘ i ' I" ” I 111 ‘Tn 1.... 1*Tu—nnTTrumi m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

0104BA.D SCAN508.M Mon Jan 28 09:50:07 2002 Page 13

NYC-WTC_000050731

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NYC-WTC_000050731Source: NYC Law Department, mirrored locally

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