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GCMS analysis results for sample AE00365, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.

NYC-WTC_000051685–000051696

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00365.D Vial: 3 Acq On : 15 Jan 2002 11:52 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 4 2-CYANOCARBAZOLE $$ 9H-Carb... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.12 ug/L 58129 Phenanthrene-dl0 22.63 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 2 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 3 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 Abundance Scan 1656 (22.280 min): 00365.D (-) m/z 192.10 100.00% 192

5000

................. /............. ) ■ ■ i ■ ■ ' ■i ■ ■ ■ ■ TT । r । l11 ' 1 96 146 22.00 22.20 22.40 22.60

n/z-> 44 70 82 O---H -PPPPT | ■ । I ■ | ■ m ' ' । । | । । । । |T1! ! | I I I I | I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 —l160 II m/z 146.10 15.58% Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 102

5000 11P 111l । 'n 22.00 22.20 22.40 22.60 m/z 193.10 15.42%

ok 9 138 T " I " " I ' " 1 1 " 1 ' I ' " ' r " ' I " ' ' I " " PTIT’ i i | | m l*| i i i i । । i । । | | I I । | i i i i । ) I i i | Tyn /z- > 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192 JI 22.00 22.20 22.40 22.60 108 5000 m/Z96.00 15.40% 146 175

Of “‘IB001—n0umBUIDTTTT TTTT’I I I ! I | IT'! I | I I ' I ' " ‘ I " " I ' rrrp n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS ' ■ i ' ' ' ■ i ■ ' 1 ' 1 ' 1 ' 1 I 192 22.00 22.20 22.40 22.60 m/z 191.10 13.97%

5000

96 164 1 138 0 " 11" ' ir " ' i " " i ■ " ■ r ' " i " '' i " " rrrri 111111 ti 1111111111111 I ' ' ' ' I ' ' ' ' I ’ 1 n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22,00 22.20 22.40 22.60

)0365.D SCAN508.M Wed Jan 16 08:13:47 2002 Page 6

NYC-WTC_000051694

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