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GCMS analysis results for sample AE00365, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.

NYC-WTC_000051685–000051696

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051695
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NYC 9/11 Public Portal Document

Data File : C : \MSDCHEM\1\5973N\02JAN15\00365 . D Vial: 3 Acq On : 15 Jan 2002 11:52 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

22.77 0.33 ug/L 154839 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 80 3 Anthracene-dlO- 188 C14D10 001719-06-8 80 4 Anthracene-DlO 188 C14D10 000000-00-0 74 Abundance Scan 1699 (22.771 min): 00365.D (-) m/z 188.10 100.00% 188

5000

80 94

m/z-> 30 40 49 66 , , 0 ----- 11PPIPWPTPPTTTTT 40 132 156 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 —l 22.40 22.60 22.80 23.00 23 20 m/z 94.05 16.89% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ z 80.05 16.10% 66 O- TIIPWWTTVTTTTTTTT n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188 , । , i । i 'l , > i ry r, i TT”i . , , । . 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.20 15.09%

80 94 160 66 - . .............. O —mmmTTTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- ' i ■ ' ' ' i ' f ■ r I 1 ■ 1 ■ I ' 1 ' ' i ' 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 13.83%

5000

. 80 94

n/z-> OF ....... l.... L 30 40 50 60 70 80 66 । i11' ■ i i "ilk "i 160

90 100 110 120 130 140 150 160 170 180 190 „10—. ----- 22.40 22.60 22.80 23.00 23.20

00365.D SCAN508.M Wed Jan 16 08:13:47 2002 Page 7

NYC-WTC_000051695

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NYC-WTC_000051695Source: NYC Law Department, mirrored locally

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