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GCMS surrogate recovery results for sample AE00280, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.

NYC-WTC_000050893–000050911

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050909
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN09\280.D Vial: 5 Acq On 9 Jan 2002 9:31 pm Operator: ' Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.24 ug/L 203978 Phenanthrene-dl0 22.65

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 94 2 Anthracene-D10 188 C14D10 000000-00-0 72 3 Anthracene-dlO- 188 C14D10 001719-06-8 56 4 Phenanthrene-diO_________________ 188 C14D10 001517-22-2 50 Abundance Scan 1699 (22.771 min): 280.D (-) m/z 188.10 100.00% 118 fl 5000 94 I 80 "F T

m/z-> 42 54 66 01 ...... . .... ... . i ■ ■ ‘ • l + 132 146 158 'i ..........i'i ■. i'H....... 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 L. 22 40 22.60 22.80 23.00 23.20 m/ z 94.10 19.71% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 .... ............ , 22.40 22 60 22.80 23.00 23.20 80 94 m/z 189.10 16.90%

m/z-> 0- 66 — r ■ " i " ' ■ i ■ " ■ i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 ..... I......... l— Abundance #84498: Anthracene-D10 188 r. 22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 15.81% 80 94 66 160 |

n/z-> 0- — ■ ■ i " ■ ■ i111111 ■' ■ i i ■ ■ " i1 ■ ■ ■ i'' ■ ■ i T‘ rr 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 mm Abundance #84502: Anthracene-d10- ..... ....... ....... 118 22.40 22.60 22.80 23.00 23.20 m/z 80.00 14.45% ft 5000

80 94 160 m L 66 n/z--> 0 ■। 40 ■ i ■ 50 1111.111/111800 i ■ ■ ■ ■ i • • ■ • i • • • ■ i 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ---------------------I- 22.40 22.60 22.80 23.00 23.20

280.D SCAN508.M Thu Jan 10 11:51:56 2002 Page 12

NYC-WTC_000050909

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NYC-WTC_000050909Source: NYC Law Department, mirrored locally

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