GCMS analysis results for sample AE00556, Feb 2002

NYC 9/11 Public Portal Document —— 2

Data File : C:\MSDCHEM\1\5973N\02JAN29\00556.D Vial: 3 . Acq On : 29 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.37 ug/L 275019 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 78 3 Phenanthrene-diO 188 C14D10 001517-22-2 64 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 47 Abundance Scan 1699 (22.771 min): 00556.D (-) m/z 188.15 100.00% 188

5000

80 94 "d T T T 44 54 66 'i111 iri ।.. ।. hr ----- I 132 160 I L 22.40 22.60 22.80 23.00 23.20 m/z 80.10 19.19% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ z 94.10 17.58% 66 .158 ■ i • ■' ■ i ■ ■ ■ ■ i • ■ । ■ i ■ ■ • ■ I ■ mmH — m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 2 TT 7 I" 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.20 15.33%

80 94 160

/z-> ■ i • ■ ■ ■ i. 40 50 6 . 1. 1.., r " ' r " ' i'' " i 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I"ll|....... 1004—— Abundance #84499: Phenanthrene-d10 "F LT 1(18 22.40 22.60 22.80 23.00 23.20 m/z 184.10 9.82%

5000

80 94 160 66 " i'''' i " ' ■ r ' । ■ i " — I' " ' I' " ' I'''' I 'I III..... 1894l.... m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

30556.D SCAN508.M Wed Jan 30 09:01:58 2002 Page 13

NYC-WTC_000051565