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GCMS analysis results for sample AE00556, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.

NYC-WTC_000051549–000051566

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document LlDrary search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN29\00556.D Vial: 3 • Acq On : 29 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 N-perdeuteriobenzylideneani... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 109750 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 Myristicine 192 C11H1203 000000-00-0 58 3 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 6-Methoxy-2,4-dihydroxy-1,5-naph... 192 C9H8N2O3 000000-00-0 50 Abundance Scan 1656 (22.280 min): 00556. D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 .m 22 00 22.20 22.40 22.60

m/z-> 42 52 64 TTHTT | T*utmn . " I 1 " 1 I 1 ' । I | I I I । | ! I t-1'| I I | I | | | It[I I I I | I I

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 118 .... . ...... I.... JU m/z 191.10 16.51% Abundance #88409: N-perdeuteriobenzylideneaniline 19 2

— 5000 82 ‘ ' i 22.00 22.20 22.40 22.60 54 m/z96.10 16.41% 110 30 I 94 160 ""I............. ' ■ | " I' PHP —IIn—mn*00m09u9——n—mpupT Tryn m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102653: Myristicine 192

22.00 22.20 22.40 22.60 5000 m/z 193.10 14.10%

91 165 "........ I 65 ■ i' I1'-' i' 77 11' | 103 T1 131 147l IL TTTTyrTTTp-rTTyrTTTp-rTTyrrrrp-rrTy'n-T-^^ II ll..... 111 •' I" n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192 22.00 22.20 22.40 22.60 m/z 146.10 13.18%

5000

144 177 " i " " r "111 ■ ■11" " i " " r ■' ■ i " ■' i " " i " " I "111" " 11111111 mp 11 11 "I m n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

0556.D SCAN508.M Wed Jan 30 09:01:58 2002 Page 12

NYC-WTC_000051564

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NYC-WTC_000051564Source: NYC Law Department, mirrored locally

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