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GCMS analysis results for sample AE00108, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.

NYC-WTC_000050754–000050773

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050772
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 ■ Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************************* * * * * ** * * Peak Number 13 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.38 ug/L 275151 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 90 3 Anthracene-D10 188 C14D10 000000-00-0 86 4 Acridine-D9 188 C13D9N 000000-00-0 45 Abundance Scan 1699 (22.771 min): 00108.D (-) m/z 188.15 100.00% 188

5000 94 -- 80 40 52 66 . 132 160 1801 22.40 22.60 22.80 23.00 23.20 mPTHPT ...... .1 ■ ■ . I ■ ■ . . I ■ . I 1-1 ■ ■ ■ ■ l ■ ■ ■ ■ | » I m/z94.05 20.85% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

........... (................................ 5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.10 16.94%

/z-> 66 TOO—/017TTT""TICITTT 1 1 i • M 1 i ' 1 1 1 1 1 1 i 1 1 1 ' i" 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 15..... Ie.. Abundance #84502: Anthracene-d10- 1(18 IPPP 22.40 22.60 22.80 2300 23.20 5000 m/z 189.10 15.84%

. 80 94 160 66 । । .> p i.i|.i. IpJ.।.m|iiii|IL • | H I I | I I I I | I l p .189.!. miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 1 111’ 11" T'. 1. "t. I"1' 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 11.41%

5000 80 94 66 160 III ■ i ■ ■1 ■ ।'1111111 ■ ।1 mmmmmmmmmmmmmmmmmmmmmmm T‘" ' i 1 ' ■ 1 i ' ' TTTTT m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

00108.D SCAN508.M Mon Jan 28 09:50:00 2002 Page 15

NYC-WTC_000050772

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NYC-WTC_000050772Source: NYC Law Department, mirrored locally

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