GCMS results for sample AE00560, Jan 17 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00560.D Vial: 4 Acq On : 15 Jan 2002 4:00 pm Operator: • Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 72702 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole ... 192 C13H8N2 057955-18-7 72 3 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 59 Abundance Scan 1656 (22.280 min): 00560.D (-) m/z 192.10 100.00% 192

5000 / \ 96 146 160 T ‘‘‘‘V 66 82 22.00 22.20 22.40 22.60

m/z-> 0- ■ I ■ > 1 ■ । > । > ■ 111 > > 111 ‘T 60 70 80 — 90 100 110 120 130 140 150 160 170 180 190 । ■1 ■ ■ । Aw 200 m/z 96.00 18.18% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 193.10 18.17% 138

m/z-> 0- ' i ■ ■ ■ • i' •' • i ■1 ‘ ■ i ■ 60 70 80 90 ----- L L 100 110 120 130 140 150 160 170 180 190 200 111111 111

Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 J 22.00 22.20 22.40 22.60 5000 m/z 191.10 15.35% 4 /z-> 0 ........... I...... ..... ................... lit 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ • i •

Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192 22.00 22.20 22.40 22.60 m/z 146.10 13.59% 108 5000

146 175

0 । ■ i■■ ■■ i L. _A l ’ ' I T m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

)0560.D SCAN508.M Wed Jan 16 08:14:10 2002 Page 9

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