Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
NYC-WTC_000050825–000050837Folder label: “GCMS X 1/7/02 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN09\0107BLA.D Vial: 1 Acq On 9 Jan 2002 5:19 pm Operator: ■ Sample : lab blank 1/7 a Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 1-Cyanocarbazole $$ 9H-Carb... Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.13 ug/L 86311 Phenanthrene-dl0 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 083415-88-7 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 64 3 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 52 Abundance Scan 1656 (22.280 min): 0107BLA.D (-) m/z 192.10 100.00% 192
5000
TI" 82 + 96 146 160
m/z-> 49 66 0 | i'| i i ■> ( FTPPD '| I It 40 50 I । I | ! I I I | I I I I | I I I I | । । ' I | ' >'l I | I I . I । . I . . | .
60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l— 22.00 22.20 22.40 22.60 m/z 193.10 16.61% Abundance #103423:1-Cyanocarbazole $$ 9H-Carbazole-1 -carbonitrile (CAS 192
5000 22.00 22.20 22.40 22.60 m/z 191.10 14.38% 96 164 OTT - 138 I' 1 ' ' I'' ' ' I - I I " " 11‘ ‘I’M . I, I.... m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 22.00 22.20 22.40 22.60 5000 m/z 96.00 13.78%
96 164
n/z- > 0 40 ‘1’11111121111111" — ..................... 1...........1 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TTT
Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS — 192 22.00 2220 22.40 22.60 m/z 146.10 12.63%
5000
96 164
m-s 40 50 60 70 80 A 138 mPPTT 90 100 110 120 130 140 150 160 170 180 190 200 X A ‘ I 1 22.00 22.20 22.40 22.60
0107BLA.D SCAN508.M Thu Jan 10 11:51:32 2002 Page 8
NYC-WTC_000050836
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NYC-WTC_000051674
Laboratory report showing GCMS blank analysis results for sample AE00365 conducted between January 15 and 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050627
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on February 4-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052233
Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003425
Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003503
Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050813
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050814
Fragmented page from a DEP laboratory record showing method parameters and sample data fields for January 7-9, 2002 testing.
Filed in the same folder
NYC-WTC_000050817
Technical form detailing GCMS analysis results for sample AE00277 listing detected compounds and concentrations from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050821
Reference report for GCMS analysis of sample AE00277 listing compound names and qualifier values from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
Filed in the same folder