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GCMS blank results for sample AE00277, Jan 2002

Machine-extracted title · confidence 90%

Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.

NYC-WTC_000050825–000050837

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050835
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN09\0107BLA.D Vial: 1 Acq On 9 Jan 2002 5:19 pm Operator: Sample : lab blank 1/7 a Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Ethane, 1,1’-oxybis[2-chlor... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

9.25 0.16 ug/L 64981 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane, 1,1’-oxybis[2-chloro- (C... 142 C4H8C12O 000111-44-4 33 2 Methane, bis(2-chloroethoxy)- 172 C5H10C12O2 000111-91-1 33 3 BIS (2-CHLOROETHOXY) METHANE 172 C5H10C12O2 000000-00-0 33 4 s-Dichloroethyl ether 142 C4H8C12O 000111-44-4 33 Abundance Scan 515 (9.254 min): 0107BLA.D (-) m/z 93.00 100.00% 93 63

5000 132

43 86 9.00 9.20 9.40 9.60 0 11 '' ' ' I ' '' ' I' I ''' I ' ' ' ' I' •i'’' ■ i f । ।। Tr m/z 63.00 68.12% ■n/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #37351: Ethane, 1,1'-oxybis[2-chloro- (CAS) $$ Bis(2-chlor... 93 63 \ 5000 A 111 > > 111 <1 9.00 9.20 9.40 9.60 27 m/z 132.00 47.63% 49 106 142 0 TIPPTIIITIITT ....... Ip i ■ ■ • ■ i 1111111'111111111111111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #75292: Methane, bis(2-chloroethoxy)- 93 63 .................... ft 9.00 9.20 9.40 9.60 5000 m/z 95.00 33.01% 27 123

49 106 171 0 ■ i'i ■ " ■ r ■' 'i' ■■■i " ■ ■ i ■ ......... ''I' TTTNTT T111 T‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #75298: BIS (2-CHLOROETHOXY) METHANE 93 9.00 9.20 9.40 9.60 m/z 65.00 29.54% 63

5000

123 49 73 106 171 oV ■ i' ■ ■ ■ r '' ''i ■ ■' ■ i1 'i'" l •"................ TT+11i ।‘। ■. • < ।. •>•।• ■ ■ ■ । >f'■। ■ m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 9.00 9.20 9.40 9.60

0107BLA.D SCAN508.M Thu Jan 10 11:51:32 2002 Page 7

NYC-WTC_000050835

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NYC-WTC_000050835Source: NYC Law Department, mirrored locally

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