GCMS blank analysis results for sample AE00110, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB04\0204BB.D Vial: 1 Acq On : 4 Feb 2002 10:58 am Operator: Sample : lab blank l/4b Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 4-Chloro-3-methylbut-2-en-l-ol Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 4.63 0.09 ug/L 40007 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Chloro-3-methylbut-2-en-l-ol 120 C5H9C10 053170-97-1 23 2 3-Penten-2-ol $$ .alpha.,.gamma.... 86 C5H10O 001569-50-2 17 3 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 9 4 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 9 Abundance Scan 110 (4.629 min): 0204BB.D (-) m/z 71.10 100.00% 41 71 88 57

5000 207

0- i (»1111... >y.. ‘ 1‘**1‘1**2*441* 1u0—2*mm—“mBBn*n000mmur n/z-> :20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundances #18624:4-Chloro-3-methylbut-2-en-1-ol 7h

5000 39 56 84 4.20 4.40 4.60 4.80 5.00 27 m/z 88.00 78.29%

m/z—> 0 JU| TIun—n—uuon)"“Bnu“C—PmgTT102 2030405060 70 8090 100110120130140150160170180190200210 120

Abundance #4047: 3-Penten-2-ol $$ .alpha., gamma.-Dimethylallyl alco... 43 71 j » * * > i > > * * । • i * < < * । * 4.20 4.40 4.60 4.80 5.00 5000 m/z 57.10 70.00% 27 53

86

n/z—> 0- . jasil 1... ।.. 1. ।.... ।..., । > ■.. ।..., (>. i 111111111 > 11, r> r| 11 n 11111111111 u 111 h r

20 30 40 50 60 70 80 90 100110120130140150160170180 190 200 210 Abundance #4072:2-Buten-l-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... i ■ '1 ■ i ■ > ■ ■ । ■ 1 • । • i ■ ’ • 71 4.20 4.40 4.60 4.80 5.00 m/z 43.10 40.77% 5000 27 39 53

86 0- kmmmmmm m/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210

•204BB.D SCAN508.M Tue Feb 05 09:47:45 2002 Page 4

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