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← Document results/DEP Box 12/GCMS X 1/20/02 A 2/25/02
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GCMS blank analysis results, Feb 25-26 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.

NYC-WTC_000003425–000003443

Folder label: “GCMS X 1/20/02 A 2/25/02”

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Scanned page image, NYC-WTC_000003431
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\0116B.D Vial: 1 . Acq On : 25 Feb 2002 11:14 am Operator: Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method-: C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Propane, 1,1-dimethoxy-2-me... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.92 0.07 ug/L 22985 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propane, 1,1-dimethoxy-2-methyl-... 118 C6H14O2 041632-89-7 9 2 Isothiocyanatoacetaldehyde dimet... 147 C5H9NO2S 075052-04-9 9 3 ISOBUTYRALDEHYDE, DIMETHYLACETAL... 118 C6H14O2 000000-00-0 9 4 ISOBUTYRALDEHYDE, DIMETHYLACETAL... 118 C6H14O2 000000-00-0 9 Abundance Scan 48 (3,916 min): 0116B.D (-) m/z 75.00 100.00% 75

5000 87 55 * • l ‘ ‘ * I ‘ ‘ ‘ I ‘ ‘ 4 I ‘ ’ I 41 t 3.60 3.80 4.00 4.20 0- TTUIDTuT । ।, 11.1.... j.... ।.... p ... ।.... (.... ।.... ।.... ।.... ।.... ।.... । 207 . m/z 87.00 41.33% ‘‘‘‘I niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200210 Abundance #17844: Propane, 1,1 -dimethoxy-2-methyl- $$ Isobutylaldehy... 75

... . .. 5000 87 3.60 3.80 4.00 4.20 m/z 55.10 32.87% 31 55 ov x +pthmmppgpITTTTT ‘I‘*IUL—COOUTNATTT- niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #42999: Isothiocyanatoacetaldehyde dimethyl acetal 75 3.60 3.80 4.00 4.20 5000 m/z 47.00 18.19% 31 47 15 58

iz-> 0-Nmp .. ....... 1 +8s101.= 10 2030405060 70 8090 100110120130140150160170180190200210 Abundance #17847: ISOBUTYRALDEHYDE, DIMETHYLACETAL $$ 1,1-Dimethoxyi... *1** 18,8 I ■ 1 ■ • i ■ ■ ■ ■ i 75 3.60 3.80 4.00 4.20 m/ z 41.10 10.79%

5000 87 55 ....... A 31 01′0099110101111111117 HttmmmpmgTTPTITTTPI niz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 3.60 3.80 4.00 4.20

0116B.D HP022102.M Tue Feb 26 08:30:41 2002 Page 4

NYC-WTC_000003431

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NYC-WTC_000003431Source: NYC Law Department, mirrored locally

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