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GCMS analysis results for sample AE00365, Jan 2002

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Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.

NYC-WTC_000051685–000051696

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051693
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00365.D Vial: 3 Acq On : 15 Jan 2002 11:52 am Operator: • Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-Pentanol (CAS) $$ Diethyl... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

9.86 0.11 ug/L 30607 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol (CAS) $$ Diethyl carb... 88 C5H12O 000584-02-1 4 2 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 3 3 1-Propanamine 59 C3H9N 000107-10-8 3 4 Guanidine $$ Aminoformamidine $$... 59 CH5N3 000113-00-8 3 Abundance Scan 568 (9.858 min): 00365.D (-) m/z 59.10 100.00% 59

5000 AA 45 1 ■ i ■ ' ■ i 1 ' 73 9.60 9.80 10.00 10.20

n/z-> — 4 O+ ■ • i11 • ■ i ■ 4 84 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 " i ■" TT7 । ■ t ■ ■ - ■ । ■ ■ । > ■ ■ ■ i ■ ■ > 11 ■ ■ ■«i ■1 ■ > i • • m/ z 45.10 20.98% Abundance #4877:3-Pentanol (CAS) $$ Diethyl carbinol $$ 3-Pentyt al... 59

5000 9.60 9.80 10.00 10.20 45 m/z 43.00 12.94% 69 73 56 I I 871111. ।। ■ 01 ' I ' " ■ | । | 1 1 1 > | ■ rri | . i > . ........ . I ।' 111111 > 1111। rn/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #500: 2-METHYL-3.3-D2-AZIRIDINE 23 58 TTT 9.60 9.80 10.00 10.20 5000 m/z 73.00 12.32%

42

n/z-> ol —ll 20 25 26

30 ........ ...... ......................... 35 40 45 50 55 “IPumumuuTOuTuu 60 65 70 75 80 85 90 95 Abundance 33 #653:1 -Propanamine 4044,. - 9.60 9.80 10.00 10.20 m/z 83.90 2.47% 5000 vv A 59 27 0 TU‘ ++++ +Hr ■ 1137■ ■ ■ I 42■ 1111 ■ < ■, I ■ ■ ■ ■ 56, 11 ■ t ' > i ■ ■ ■ • i > > • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । ■ i ■ • • ■ i ■ ■ ■1 i '1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 9.60 9.80 10.00 10.20

00365.D SCAN508.M Wed Jan 16 08:13:47 2002 Page 5

NYC-WTC_000051693

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NYC-WTC_000051693Source: NYC Law Department, mirrored locally

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