GCMS analysis results, sample AE01139, 2,4-DDD, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01139.D Vial: 5 Acq On : 25 Feb 2002 2 :32 pm Operator: ' Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 1-Propanamine (CAS) $$ n-Pr... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

9.90 0.12 ug/L 36344 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 4 2 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 4 3 Acetaldehyde, (3,3-dimethylcyclo... 152 C10H16O 026532-25-2 4 4 1-Propanamine 59 C3H9N 000107-10-8 3 Abundance Scan 578 (9.899 min): 01139.D (-) m/z 59.00 100.00% 59

5000

44 01 ' i1 ■ ■ ‘ i 11 ■ ■ i111 ■ i' ..... I, X 73

‘ i 1 ■ ■ ■ i ■ ' 84 7172/2/2.1 152

7’1 N M 9.60 m/z 151.90 ■ ' i ' ' ' ' i ■ ■ 9.80 10.00 10.20 19.92% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #654:1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine... 59

5000 42 9.60 9.80 10.00 10.20 m/z 73.00 16.92% Of ■ i ■ ■ ■ ■ i ■1 ' i 1 1 ■ ■ 1 ' 1 1 ' i 1 i 1 ' 1 1 i ■ ■ 1 ' i /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150

A..... Abundance #500: 2-METHYL-3.3-D2-AZIRIDINE 29 58

9.60 9.80 10.00 10.20 5000 m/z 83.90 15.92%

42 fl fl W A A, mz-> o 20 30 l 40 50 t1"111111111111111111111111111' i1 ■ ■ ■ i ■ ■ ■11' ■ ■ ■ । 60 70 80 90 100 110 120 130 140 150 ■1 ■ ।

Abundance #49640: Acetaldehyde, (3,3-dimethylcyclohexylidene)-, (E)-... 41 9.60 9.80 10.00 10.20 m/ Z 44.00 14.53% 109 5000 137 152 J A A A A 93 119 84

0- TI2111/T11111-10--"t1‘171111T11- > > i ■ ■ ■ ■ i * । । ' i ■ । • i 1′1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 9.60 9.80 10.00 10.20

01139.D HP022102.M Tue Feb 26 08:30:11 2002 Page 10

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