NYC-WTC_000003503
Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results, sample AE01139, 2,4-DDD, Feb 2002
Machine-extracted title · confidence 92%Gas chromatography-mass spectrometry analysis report for sample AE01139 detecting surrogate 2,4-DDD at 76 ug with MDL of 5.0, analyzed on 02/27/2002.
NYC-WTC_000003483–000003502Folder label: “GCMS X 1/20/02 A 2/25/02”
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OCR text
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NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02FEB25\01139.D Vial: 5 ■ Acq On : 25 Feb 2002 2:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Methyl-d3-hydrazine sulfate Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
12.45 0.03 ug/L 12940 Naphthalene-d8 13.20
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Methyl-d3-hydrazine sulfate 49 CH3D3N2 000000-00-0 3 2 cis-15-methoxycarbonyl-3-ethenyl ... 368 C16H20N2O4S2 112792-86-6 2 3 trans-2,5-dimethoxycarbonyl-3-et... 368 C16H20N2O4S2 112792-87-7 2 4 chloromethyl acetate $$ Chlorome... 108 C3H5C1O2 000625-56-9 2 Abundance Scan 804 (12.450 min): 01139.D (-) m/z 49.00 100.00% 49
84 MMNWaAAWWNA 5000
12.20 12.40 12.60 12.80 0— ■ ■ r ■ ■ ■ i T‘utI1E1111"31110--I1TCETT-T/TT"T"‘IIIIIT m/z 84.00 66.59% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #281: Methyl-d3-hydrazine sulfate 49
5000- 1 ■ i 1 ■ ■ I ' • 1 I ‘ ' 12.20 12.40 12.60 12.80 m/ z 44.00 63.06%
Tl/Z-> 0- JI 40 TIn’n—In001—000-0B011111mu’n-0’’’010003311011111 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 mH A
Abundance #311745: cis-15-methoxycarbonyl-3-ethenyl-4-benzylthio-1,2... 49 84 ' ' I ' 1 I 1 ' ' ( I ' * ' I l 1 ■ 12.20 12.40 12.60 12.80 5000
368 0 11 ■ " 11 " i T’I—IB0’m0110011—00—1—IOTIItT IIII i ■ ‘ " i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #311746: trans-2,5-dimethoxycarbonyl-3-ethenyl-4-(benzylth... 49 84
5000
368 0 ■ ।1 > ■ ■ i ■ ■ ■ ■ । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
01139.D HP022102.M Tue Feb 26 08:30:11 2002 Page 11
NYC-WTC_000003497
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NYC-WTC_000003497Source: NYC Law Department, mirrored locally
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