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GCMS analysis results, sample AE01139, 2,4-DDD, Feb 2002

Machine-extracted title · confidence 92%

Gas chromatography-mass spectrometry analysis report for sample AE01139 detecting surrogate 2,4-DDD at 76 ug with MDL of 5.0, analyzed on 02/27/2002.

NYC-WTC_000003483–000003502

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01139.D Vial: 5 Acq On : 25 Feb 2002 2 :32 pm Operator: ■ Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.11 ug/L 50099 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 3 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C2 0H4 005Si4 000000-00-0 37 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 37 Abundance Scan 812 (12,540 min): 01139.D (-) m/ z 73.00 100.00% 73

5000 267 355 ... H... 12.20 12.40 12.60 12.80 45 — । i 0- ■i' m/z 266.90 44.76% n/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 - 267 5000 12.20 12.40 12.60 12.80 m/Z 355.10 38.90% 207 I 323 I 0— 1 i ' ■ 1 1 1 1 1 1 I ----------- m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

12.20 12.40 12.60 12.80 5000 267 m/ z 356.00 15.00% 355 45 193 0- I i • i ' 233.104011/1 323 TLl m/z-> 50 100 150 200 250 300 350 400 450 Abundance #361636: 3,4-DIHYDROXYMANDELIC ACID-TETRATMS ' ' i ' ■ ' 1 1 1 1 ■ i ' ' ■ ■ i ■ ■ ■ • i 73 12.20 12.40 12.60 12.80 m/ Z 2 68.00 12.62% 355 5000

45

m/z-> 0 Td 50 | | 100 4 150 193 200 267 295 250 300 350 [ 400 429 457 450 ' ■ i ' 1 ' ' I X...... 12.20 12.40 12.60 12.80

01139.D HP022102.M Tue Feb 26 08:30:11 2002 Page 12

NYC-WTC_000003498

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NYC-WTC_000003498Source: NYC Law Department, mirrored locally

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GCMS analysis results, Feb 27 2002 · Box DEP Box 12

NYC-WTC_000003463

Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998

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