NYC-WTC_000003503
Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results, sample AE01139, 2,4-DDD, Feb 2002
Machine-extracted title · confidence 92%Gas chromatography-mass spectrometry analysis report for sample AE01139 detecting surrogate 2,4-DDD at 76 ug with MDL of 5.0, analyzed on 02/27/2002.
NYC-WTC_000003483–000003502Folder label: “GCMS X 1/20/02 A 2/25/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02FEB25\01139.D Vial: 5 Acq On : 25 Feb 2002 2:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4(1H)-Pyrimidinone, 2-amino.. Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.04 ug/L 17008 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4 (1H) -Pyrimidinone, 2-amino-6-(m. . . 140 C5H8N4O 054004-20-5 9 2 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N2O2 004212-49-1 9 3 5-Fluoronicotin amide 140 C6H5FN20 000000-00-0 9 4 l-ETHYL-4,5-DIMETHYL-4-IMIDAZOLI... 140 C7H12N20 059167-88-3 9 Abundance Scan 886 (13.376 min): 01139.D (-) m/z 140.00 100.00% 140
5000
70 44 13.00 13.20 13.40 13.60 13.80 ....... ........................ || m/z 70.00 01 ■ > i ■ - ■ > i - > ■ ■ i ■ । 1 20.95% m/z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #35078:4(1 H)-Pyrimidinone, 2-amino-6-(methylamino)- 140
44 5000- 13,00 13.20 13.40 13.60 13.80 111 70 82 m/z 68.00 14.97% 97 .
mfe-> ol ■ ' i ■ 40 50 60 70 80 ■ 1 i 90 100 ....... 1I ql l......... 14 1 1 I I I 1 I I l‘l I I I I I I I I I I I 110 120 130 1 140 111
Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 82 13.00 13.20 13.40 13.60 13.80 5000- m/z 44.00 13.84%
54 68 96
miz- > 01 1 1 1 1 1 ■ ■ i ■ 40 50 1 1 I 1 1 1 1 I 1 11 1 1 90 | 111 i'' > । । 1 1'> l 1 - ■ । i'i > > । । i i 100 110 120 + TIT 60 70 80 130 140 Abundance #35137:5-Fluoronicotin amide TIT ■ ' । . ‘I . Tk" 1-0 13.00 13.20 13.40 13.60 13.80 m/z 141.00 13.49% 96 5000 124 44 69 76 50 —
m/z-> 0 118 40 IT.... 50 60 70 ■ i ■ ■ ■ > i ■ ■ 80 90 I 100 110 120 130 | 140 T1d 13.00 13.20 13.40 13.60 13.80
01139.D HP022102.M Tue Feb 26 08:30:11 2002 Page 13
NYC-WTC_000003499
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NYC-WTC_000003499Source: NYC Law Department, mirrored locally
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