GCMS analysis results, sample AE02719, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report ** Data File : C:\MSDCHEM\l\5973N\02FEB28\02719.D Vial: 4 Acq On : 28 Feb 2002 5:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 4(1H)-Pyrimidinone, 2-amino... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.07 ug/L 33466 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4 (1H) -Pyrimidinone, 2-amino-6-(m. . . 140 C5H8N40 054004-20-5 9 2 5-Fluoronicotin amide 140 C6H5FN2O 000000-00-0 9 3 3H-Pyrazol-3-one, 2,4-dihydro-2 ,... 140 C7H12N20 003201-25-0 9 4 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 9 Abundance Scan 886 (13.376 min): 02719.D (-) m/z 140.00 100.00% 140

5000 ...................... I\......................... 70 13 00 13.20 13.40 13.60 13.80 0- ' • l • ' ■ ' I ‘ ‘ ‘ l ‘ —1 1....... ■ • ‘ ■ i m/z 70.00 14.07% n/z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #35078:4(1H)-Pyrimidinone, 2-amino-6-(methylamino)- 140

44 5000 • i ■ 1 18iT 1 1 1 1 ' ■ ' i ■ 13.00 13.20 13.40 13.60 13.80 111 70 82 m/z 141.00 10.17% 97 , 0- ■ ' i ■ ■ * । ■ • ■ ■ । • ■ I ■ ' ■ • i 1 ti, , , , Ill, ......... ...... II II m/z-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #35137:5-Fluoronicotin amide 140 96 ' i 1 1 1 ' i 1 1 ' ■ i ■ ■ ■ ■ i ■ 13.00 13.20 13.40 13.60 13.80 5000 124 m/z 136.10 5.12% 44 69 76 50 0- ■ ■ i ■ ----- —1 TB.F nz-> 40 50 60 70 80 90 100 110 120 130 140 Abundance #35412:3H-Pyrazol-3-one, 2,4-dihydro-2,4,4,5-tetramethyl-... 41 140 13.00 13.20 13.40 13.60 13.80 69

5000 97

125 , 82

iz-> 0- 111 1 40 53 1 1 i'1' I । । । ■ । I 50 60 70 Ip 80 90 11-mTgTT 1 "I-I—r 100 110 120 130 140

02719.D HP022102.M Fri Mar 01 10:07:35 2002 Page 11

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