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GCMS analysis results for sample AE00108, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.

NYC-WTC_000050754–000050773

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050770
OCR text

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NYC 9/11 Public Portal Document ** I —*L -

Data File : C: \MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 • Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Cyclopentasiloxane, decamet... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.06 ug/L 42117 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83 3 Noradrenaline tetraTMS 457 C20H43N03Si4 068595-65-3 37 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 803 (12.541 min): 00108.D (-) m/z 73.10 100.00% 73

5000 267 355

12.20 12.40 12.60 12.80 49 । m/z 267.00 40.61% m/z-s 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 TTTTTTrmi 12.20 12.40 12.60 12.80 355 m/z 355.10 35.04% 45 I I 193 223 . 323 L TUUTTTTTTTTTTTTTTTIWWTTTTTTTTTTTTTTTTTTT M | .... | ...Ji.lll...T, . | .... | ....p.. I p I I m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 12.20 12.40 12.60 12.80 267 m/z 356.10 12.25% 5000

207 323 . TTCmTTTTTTT1*1”**T****ITTT1T TPWTTTTTTTT WWWTmRPTTTT m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #357156: Noradrenaline tetraTMS I 'r' 'T '. r 1'1' 73 12.20 12.40 12.60 12.80 m/z 268.00 11.13%

5000 102 355

45 i 147 442 ‘I’’’’* ‘TTTTTTTTTTTTTTTTTTuuuuTuuu i"’ i"r!y. 1 /z-> 40 60 80 100120140160180200220240260280300320340360380400420440 12.20 12.40 12.60 12.80

00108.D SCAN508.M Mon Jan 28 09:50:00 2002 Page 13

NYC-WTC_000050770

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NYC-WTC_000050770Source: NYC Law Department, mirrored locally

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