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GCMS blank analysis results for sample AE00027, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.

NYC-WTC_000050716–000050734

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050728
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02JAN25\0104BA.D Vial: 1 Acq On : 25 Jan 2002 10:12 am Operator: Sample : lab blank 1/4 a Inst : Inst rumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Cyclopentasiloxane, decamet... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.11 ug/L 62071 Naphthalene-d8 13.19 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83 3 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 33 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 23 Abundance Scan 803 (12.541 min): 0104BA.D (-) m/ z 73.10 100.00% 73

5000 267 355 TFT11nmmTmmuu—*1m 45 12.20 12.40 12.60 12.80 mPPP-mP । i TJ, I | * j |T|I| m/z 267.00 38.73% /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 ____________ /I 5000 ‘ ‘ I ' ' ' ' I ' 1 ' ' 1 ‘ rii r C'"1"' i1 12.20 12.40 12.60 12.80 m/z 355.10 37.43% 191207 251 1 323339 J •i111111 1111' i11 ‘ i I " " I 1M ‘I 1 '' ' I ' ‘ i | | । I। D1—uu"3—TuTT z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 T. I. ’. '. TTT. Tr T-J-T T rr. i1. ■ 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 15.03% 355 45 l 193 223 251 , 323339 । T TTTTTLUTTTTUTTTTTTTTTTTTTTTTHTUTTTTTTTTTTTTTTT’TTUuer m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #339188: N-Methyladrenaline, tri-TMS ■ ' i 1 1 ■ ■ i ■ ■ i. ■. ............1. 11 58 73 12.20 12.40 12.60 12.80 m/z 267.90 9.49%

5000 355

m/z—> M.... .. 207

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 2 . .. L 12.20 12.40 12.60 12.80

)104BA.D SCAN508.M Mon Jan 28 09:50:06 2002 Page 10

NYC-WTC_000050728

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NYC-WTC_000050728Source: NYC Law Department, mirrored locally

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