NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\O2 JAN25\0104BA.D Vial: 1
Acq On : 25 Jan 2002 10:12 am Operator:
Sample : lab blank 1/4 a Inst : Instrumen
Mise : January 25, 2002 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator)
Title : 508 scan method
Library : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 9 IH-cyclobuta[de]naphthalene... Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
16.55 0.04 ug/L 23931 Ac enaphthene -d10 18.34
Hit# of 5 Tentative ID MW MolForm CAS# / Qual
--------------- -
1 IH-cyclobuta[de]naphthalene $$ C... 140 C11H8 024973-91-9 9
2 4H-Pyran-4-one, 2-ethyl-3-hydroxy- 140 C7H803 004940-11-8 9
3 2-Dimethylamino-4,5-dimethyl-oxa... 140 C7H12N20 000000-00-0 9
4 2-DIMETHYLAMINO-4,5-DIMETHYLOXAZ... 140 C7H12N20 073777-29-4 9
Abundance Scan 1154 (16.549 min): 0104BA.D (-) m/z 140.20 100.00%
140
5000
122 172
43 89 71 16.20 16.40 16.60 16.80
T’I—unU’utmmutumm—u’u—nmuuTrrw ' r 1 | । I <. n. TT -r-rp m/z 172.20 28.20%
/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170
Abundance #36659:1H-cyclobuta[de]naphthalene$$ Cyclobuta[de]naphth...
140
5000 "1 i. '. ‘"""I"’ ' l r’.rr.ri *..। '
16.20 16.40 16.60 16.80
m/z 138.10 26.86%
7089 113
— II |
11'I'''' i111' I' 11 ‘ ’1 111,11
■ i ■ M • i ■ ■'111 ■ ■' i1'(1111
mlz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170
Abundance #35344: 4H-Pyran-4-one, 2-ethyl-3-hydroxy-
140
• ■ i ■ ■ > ■ । ■ I ’nrl .•■n । i
16.20 16.40 16.60 16,80
5000 m/z122.10 25.15%
71
97
125
55
84 | 111 1Y_________________
r.'. I. '. r . l. '.1. 'f'. I 111<'i111 ‘ TT rp i i r I i n f j l i t » } «
m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170
Abundance #35431:2-Dimethylamino-4,5-dimethyl-oxazole PIUTTTTTTT
140 16.20 16.40 16.60 16.80
m/z 71.00 17.70%
5000 44
56 111
72 125
97
|
TIT I
TWPWTTITTTTT Ttt ‘b""‘TO—B21TrrEET TTTTTrir
• • i - ■ « ■ i < ‘
m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80
0104BA.D SCAN508.M Mon Jan 28 09:50:06 2002 Page 11
NYC-WTC_000050729
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