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← Document results/DEP Box 28/GCMS X 1/4/02 A 1/25/02
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GCMS blank analysis results for sample AE00027, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.

NYC-WTC_000050716–000050734

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050729
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2 JAN25\0104BA.D Vial: 1 Acq On : 25 Jan 2002 10:12 am Operator: Sample : lab blank 1/4 a Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 IH-cyclobuta[de]naphthalene... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.04 ug/L 23931 Ac enaphthene -d10 18.34 Hit# of 5 Tentative ID MW MolForm CAS# / Qual --------------- - 1 IH-cyclobuta[de]naphthalene $$ C... 140 C11H8 024973-91-9 9 2 4H-Pyran-4-one, 2-ethyl-3-hydroxy- 140 C7H803 004940-11-8 9 3 2-Dimethylamino-4,5-dimethyl-oxa... 140 C7H12N20 000000-00-0 9 4 2-DIMETHYLAMINO-4,5-DIMETHYLOXAZ... 140 C7H12N20 073777-29-4 9 Abundance Scan 1154 (16.549 min): 0104BA.D (-) m/z 140.20 100.00% 140

5000 122 172 43 89 71 16.20 16.40 16.60 16.80 T’I—unU’utmmutumm—u’u—nmuuTrrw ' r 1 | । I <. n. TT -r-rp m/z 172.20 28.20% /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #36659:1H-cyclobuta[de]naphthalene$$ Cyclobuta[de]naphth... 140

5000 "1 i. '. ‘"""I"’ ' l r’.rr.ri *..। ' 16.20 16.40 16.60 16.80 m/z 138.10 26.86% 7089 113 — II | 11'I'''' i111' I' 11 ‘ ’1 111,11 ■ i ■ M • i ■ ■'111 ■ ■' i1'(1111 mlz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35344: 4H-Pyran-4-one, 2-ethyl-3-hydroxy- 140 • ■ i ■ ■ > ■ । ■ I ’nrl .•■n । i 16.20 16.40 16.60 16,80 5000 m/z122.10 25.15% 71 97 125 55 84 | 111 1Y_________________ r.'. I. '. r . l. '.1. 'f'. I 111<'i111 ‘ TT rp i i r I i n f j l i t » } « m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35431:2-Dimethylamino-4,5-dimethyl-oxazole PIUTTTTTTT 140 16.20 16.40 16.60 16.80 m/z 71.00 17.70%

5000 44 56 111 72 125 97 | TIT I TWPWTTITTTTT Ttt ‘b""‘TO—B21TrrEET TTTTTrir • • i - ■ « ■ i < ‘ m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

0104BA.D SCAN508.M Mon Jan 28 09:50:06 2002 Page 11

NYC-WTC_000050729

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NYC-WTC_000050729Source: NYC Law Department, mirrored locally

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