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GCMS analysis results for sample AE03249, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03249 conducted on March 15, 2002.

NYC-WTC_000006166–000006185

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006180
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C : \MSDCHEM\1\5973N\02MAR01\03249 .D Vial: 4 . Acq On : 1 Mar 2002 6:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 N-perdeuteriobenzylideneani ... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 119063 Phenanthrene-dl0 22.63 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 Pyrazine, tetraethyl- (CAS) $$ t... 192 C12H20N2 038325-19-8 50 3 1,5-Naphthalenedithiole 192 C10H8S2 000000-00-0 42 4 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H130P 000000-00-0 42 Abundance Scan 1675 (22.283 min): 03249.D (-) m/z 192.10 100.00% 1912

5000

82 96 146 160 22.00 22.20 22.40 22:60 0- 52 66 8|2 11 I— 1 1 " 1 1 I ' 1 1 1 I Tr l I I l p-i I I | Il TT I I i | l r /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 120 TTT 44,10 l m/Z 191.00 20.72% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22:60 54 m/z 96.10 15.18% 0 30 I 94 11" " i" " i1 " i11" i ■ >! I | | l pli | I n 110 160 " i " " i' " 11' " ' i "111'11111 ■ " 11" il U A m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103348: Pyrazine, tetraethyl- (CAS) $$ tetraethyl pyrazine 192

177 22.00 22.20 22.40 22.60 5000 m/ Z 146.10 13.57% A

_ _____ _______ II 53 67 81 hl______J___________________________________ 1______, I,_____ . 149 163 0 " I " " I " " I' ‘1' I''1' I' " ' I ‘" I'' " I " " 11'" 111" I "1' I'11111111111111" "11' nz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102434: 1,5-Naphthalenedithiole .... ......... A. 1912 22.00 22.20 22.40 22.60 m/z 193.00 13.44%

5000 115 128 159 147

m/z—> 0 33 mm102 . ...... 1 1" i1,111111 " i " '11" " I " " I" " I' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 ■ i1"11 ■ ■ ■ ’111 22.00 22.20 22.40 22.60

3249.D HP022102.M Mon Mar 04 12:33:35 2002 Page 11

NYC-WTC_000006180

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NYC-WTC_000006180Source: NYC Law Department, mirrored locally

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