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GCMS analysis results for sample AE00841, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052311–000052329

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052326
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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02FEB07\00841.D Vial: 4 Acq On : 7 Feb 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 10 N-perdeuteriobenzylideneani ... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 92817 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 3 l-amino-2-methyl-4-isopropyl-thi ... 192 C5H13N4PS 107264-54-0 50 4 Phenanthrene, 3-methyl- (CAS) $$... 192 C15H12 000832-71-3 42 Abundance Scan 1656 (22.280 min): 00841 .D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60

m/z—> 0 42 54 64 mTIWTTTTHHT JlLr 1 'I""I"''I1'"I' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 'I'’'1I‘'1'I■'1'I'‘ m/z 191.10 16.80% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 - 22.00 22.20 22.40 22.60 54 m/z 146.10 15.28% 0 "I.. 30 '' i1''11'''' i 94 ■'JI.. 110 160 ....... . ......... . ‘I N m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 .................... .5 22.00 22.20 22.40 22.60 5000 m/z 193.10 14.98%

96 165 88 J 139 152 176 0 Jr ........ 'I' n i1 ‘" i" " i11 ■' 1111' i" " i1" ' 111111" " I" 111" " I" "'I" 1_ri" " i m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192 22.00 22.20 22.40 22.60 m/z96.00 12.96% l| 5000

144 177 ********* 0 —PPP I ■ I’’ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

30841.D HP020702.M Thu Feb 21 09:58:03 2002 Page 12

NYC-WTC_000052326

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NYC-WTC_000052326Source: NYC Law Department, mirrored locally

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