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GCMS analysis results for sample AE00841, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052311–000052329

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052327
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NYC 9/11 Public Portal Document

PW —

Data File : C:\MSDCHEM\1\5973N\02FEB07\00841.D Vial: 4 Acq On 7 Feb 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Anthracene-D10 Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.36 ug/L 245719 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-DlO 188 C14D10 000000-00-0 90 2 Anthracene-d10- 188 C14D10 001719-06-8 80 3 Phenanthrene-diO 188 C14D10 001517-22-2 72 4 Cycloheptanone, 4-phenyl - 188 C13H16O 067688-28-2 43 Abundance Scan 1699 (22.771 min): 00841.0 (-) m/z 188.10 100.00% 188 N

5000 94 80 49 66 132 160 180 22.40 22.60 22.80 23.00 23.20 0 p i iT| r 1 T ri i p i I l'| , > i r | I , - — m/z 94.10 24.51% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188

5000 22.40 22.60 22.80 23.00 23.20 80 m/z 184.10 21.19% 94 66 160 1

m/z-> 0IPTPT 40 50 60 70 S r TTnrr 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d IQ- 188 ............ ...

22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 15.36%

94 160 66 “ 0 TTITTTTI TIT I 1 1 ' 1 I' ' ' ' I1' 1111''1 I — 10ul—. m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 ----- 188 22.40 22.60 22.80 23.00 23.20 m/z 189.10 12.47%

5000

94 80 160 66 m/z-> 0 TTPTTT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 tll.... — 22.40 22.60 22.80 23.00 23.20

)841.D HP020702.M Thu Feb 21 09:58:03 2002 Page 13

NYC-WTC_000052327

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NYC-WTC_000052327Source: NYC Law Department, mirrored locally

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