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GCMS analysis results for sample AE00844, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052291–000052310

Folder label: “GCMS X 1/11/02 A 2/7/02

Page image
Scanned page image, NYC-WTC_000052307
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 11 Anthracene-D10 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.61 ug/L 387375 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-DlO 188 C14D10 000000-00-0 91 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 86 3 Anthracene-dlO- 188 C14D10 001719-06-8 80 4 Phenanthrene-dlO 188 C14D10 001517-22-2 80 Abundance Scan 1699 (22.771 min): 00844.D (-) m/z 188.20 100.00% 188 A

5000

80 94 158 .... /1........... 49 > ■ 11 64 132 146 1 22.40 22.60 22.80 23.00 23.20 < I i ■ । > ill sosplary* 0 PTTT -H— m/z 184.10 17.48% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188

5000 22.40 22.60 22.80 23.00 23.20 80 m/z 189.15 15.73% 94 66 160 । 0 I■II'II‘ ' I 1 11 ' I ' ' ' i1 ■ ■' i'''' i ■ ■ ■ ■ i' ■'' i -PPPP . ...... n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 ---

22.40 22.60 22.80 23.00 23.20 5000 m/z 187.15 15.38%

80 94 158 , 66 0 I " 111"" i1111 r - U m/z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #84502: Anthracene-d10- 188 1 i ■ l.... ..... ' ' 1 I ' 1 1 1 1 1 ' ' ‘ I ' 22.40 22.60 22.80 23.00 23.20 m/z 80.10 14.81%

5000

/z—> — 80 94 DO 160 0 TTTPTTPPT ■ ■ i'1 ■ ■ i1 ■ ■ ■ i' ■ ■' i' ■ ■ ■ i''' ■ i ■ ■ ■ ■ i ■jh........ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 | 2 l 22.40 22.60 22.80 23.00 23.20

00844.D HP020702.M Thu Feb 21 09:58:17 2002 Page 13

NYC-WTC_000052307

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NYC-WTC_000052307Source: NYC Law Department, mirrored locally

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