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GCMS results for sample AE00561, Jan 17 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051755–000051767

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051766
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00561.D Vial: 5 Acq On : 15 Jan 2002 4:50 pm Operator: ' Sample : 508 scan Inst : Instrumen Mise 2002 : January 15, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.33 ug/L 173456 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 80 2 Phenanthrene-diO 188 C14D10 001517-22-2 80 3 Anthracene-DlO 188 C14D10 000000-00-0 64 4 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 56 Abundance Scan 1699 (22.771 min): 00561.D (-) m/z 188.10 100.00% 188

5000

66 80 94 m 22.40 22.60 22.80 23.00 23.20

n/z-> 0 40 44 TWTTTTTTTT 11 50 60 । 70 80 —H 132 Ui............ . 160 — 90 100 110 120 130 140 150 160 170 180 190 m/z 94.10 24.72% Abundance #84502: Anthracene-d10- 188

5000 - 22.40 22.60 22.80 23.00 23.20 m/z 189.15 18.60%l „ 80 94 160 । 01 ........ I....... .... ... n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188 ............ ...... ..................................

22.40 22.60 22.80 23.00 23.20 5000 m/ z 80.00 14.10%|

80 N 94 160 66

n/z-> 0 „ 1.111PT1 M ।. l. j > । 40 50 60 70 80 III...... .......... 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene- D10 ---------------------------------- 1418 22.40 22.60 22.80 23.00 23.20 m/z 184.10 11.80%

5000 80 94 66 160 । ............ . • ■ • | I I ' . | . . , . | ' . . . ( . . ' . | . I 1 1 | I 1 I I | 1 1 t- I |........ .. I ! I I | IT 0 1 rp > > 1 mr । > I 1 । > TTTnr m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

30561.D SCAN508.M Wed Jan 16 08:14:14 2002 Page 8

NYC-WTC_000051766

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NYC-WTC_000051766Source: NYC Law Department, mirrored locally

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