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GCMS surrogate recovery results for sample AE00282, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00282 analyzed on January 10, 2002.

NYC-WTC_000050932–000050947

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050945
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02JAN09\282.D Vial: 7 Acq On : 9 Jan 2002 11:12 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L **************************************************************** * * * * * Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.28 ug/L 186038 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 78 2 Phenanthrene-dlO 188 C14D10 001517-22-2 78 3 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 72 4 Acridine-D9 188 C13D9N 000000-00-0 72 Abundance Scan 1699 (22.771 min): 282. D (-) m/z 188.10 100.00% 188

5000

94 80 22.40 22.60 22.80 23.00 23.20 49274 TT > I I. I1 ' ' । । । . . . . । ' 1 < । । ' । « । .146 H | . . ■ . । » । i ।M . . 1 . । .158 Fo 66 o1 m/z 94.10 17.99% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d IQ- 188

5000 -------------------------- 22.40 22.60 22.80 23.00 23.20 m/z 189.10 13.93% — 80 94 160 0- ... y. 1. 1. l i ■ ■' ■ r " ' i''1' i m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/ z 80.10 11.72%

80

m/z-> 0- 66 IPWTTTTTTT 40 50 60 70 80 + 4 .... ............ Ill... .1891... 94 160

90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 . r r. ... 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 10.97%

5000

94 80 66 i 158 I I 0 nmPPPPTTTT TTT ----- /z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

282.D SCAN508.M Thu Jan 10 11:52:05 2002 Page 9

NYC-WTC_000050945

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NYC-WTC_000050945Source: NYC Law Department, mirrored locally

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