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GCMS results for sample AE00702, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051895–000051913

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051910
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NYC 9/11 Public Portal Document

1 *E

Data File : C:\MSDCHEM\1\5973N\02JAN16\00702.D Vial: 2 - Acq On : 16 Jan 2002 3 :57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 10 Anthracene-D10 Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.26 ug/L 164519 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-D10 188 C14D10 000000-00-0 87 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 87 3 Anthracene-d10- 188 C14D10 001719-06-8 80 4 Phenanthrene-dlO 188 C14D10 001517-22-2 56 Abundance Scan 1699 (22.771 min): 00702.D (-) m/z 188.10 100.00% 188

5000

94 -------- 80 41 57 66 | 158 — 22.40 22.60 22.80 23.00 23.20 oh----H - m/z94-10 23.17% n/z- > 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 1(18

5000 22.40 22.60 22.80 23.00 23.20 80 m/z 189.10 17.70% 94 66 160 । O- ■' J m —l|........ Tuur m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 1$8

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 14.23%

80 94 66 Of mree l | I ! I > | I I I I | I > I — ■11" " 1 ■111111111111111"11"158 I — 1H111111"' 11 II I 1. miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 22.40 22.60 22.80 23.00 23.20 m/ z 80.05 13.47%

5000

66 80 94 160 ,I Orr ' i " " i1 srelsga... ll. ........................ ll|...... . ‘IB 7m 11 । । "TT /z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

10702.D SCAN508.M Thu Jan 17 08:17:24 2002 Page 12

NYC-WTC_000051910

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NYC-WTC_000051910Source: NYC Law Department, mirrored locally

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