GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000051895–000051913Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
*— 2 ‘ ‘L
Data File : C:\MSDCHEM\1\5973N\02JAN16\00702.D Vial: 2 • Acq On : 16 Jan 2002 3:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\l-..\SC7kN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 9 2-CYANOCARBAZOLE $$ 9H-Carb... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 102670 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-CYANOCARBAZOLE $$ 9H-Carbazole ... 192 C13H8N2 057955-18-7 64 2 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 3 1,4-Dimethyl-3,5-propanobicyclo[... 192 C13H20O 000000-00-0 47 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 45 Abundance Scan 1656 (22.280 min): 00702.D (-) m/z 192.10 100.00% 192
5000
22 96 146 160 22.00 22.20 22.40 22.60 42 70 82 ,1 Of H1' Fr I" I' l''" 11...... 11' 118 I ........ "'I'i' ■ ■ 11 ■ l"T m/Z 191.10 17.27% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420:2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 1$2
5000 1 1 1,1 1 1 1 22.00 22.20 22.40 22.60 1. . m/z 96.00 14.63% 164 Ofr 86 138 >>!<>> I | . I MmT | < < . . | > > > > | < < I > | l < > > | M . I | ! < | | | I I I l*| I I J I | I • i' ■ ■ ■ i TTTp-, m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin. .. 159 192
22.00 22.20 22.40 22.60 5000 m/z 146.10 12.94%
144 177
O- ■ i • •'11' ■ ’' i ■ > ■ ■ i ■ ■ ■ • i' I'' " I'' IT I— m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103601:1,4-Dimethyl-3,5-propanobicyclo[2.2.2]octan-2-one ........... A ■ ■ i • ■ ■ ■ i ■ ■ 1 ’ k I ‘ ' 107 192 22.00 22.20 22.40 22.60 159 m/z 193.10 12.56% 119 93 5000 132 145 174
/z-> O- TT " I " " i TT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ......... .......II 22.00 22.20 22.40 22.60
30702.D SCAN508.M Thu Jan 17 08:17:24 2002 Page 11
NYC-WTC_000051909
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NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051860
GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051948
Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051697
Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder