GCMS analysis results for sample AE00247, Jan 2002

NYC 9/11 Public Portal Document **— j

Data File : C: \MSDCHEM\1\5973N\02JAN24\00247.D Vial: 3 • Acq On : 24 Jan 2002 4:38 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Anthracene-D10 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.27 ug/L 200741 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-D10 188 C14D10 000000-00-0 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 91 3 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 4 Phenanthrene-diO 188 C14D10 001517-22-2 90 Abundance Scan 1699 (22.771 min): 00247. D (-) m/z 188.10 100.00% 118

5000

94 . 80 22.40 22.60 22.80 23.00 23.20

mlz-> 42 54 66 ... ....... 1| 72 +146 — 44 , — 4 -H — . ...................................................... 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 184.10 18.11% Abundance #84498: Anthracene-D10 188

5000 -- । । ■ * ■ < । ■ 22.40 22.60 22.80 23.00 23.20 80 94 m/z 94.10 16.06% 66 160 | 1 -------------------------- niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188 ‘ i ■ ■ ■ ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ' i ■ 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 15.38%

80 94 160 66 niz-> ti‘ 40 I HI «I" I > I -HH i11' ■ i'1 • ■ i ■" ■ i • ■ ‘ ■ i' ■ “ i ■ 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 — 188 22.40 22.60 22.80 23.00 23.20 m/z 80.10 12.20%

5000

80 94 66 158 “ i “ ■ • i “ 1' i “1 ■ i “ 1 TTTT TTTITITI ------------- n/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

0247.D SCAN508.M Fri Jan 25 10:26:05 2002 Page 14

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