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GCMS analysis results for sample AE01142, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01142 conducted on February 27, 2002.

NYC-WTC_000003523–000003542

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01142 .D Vial: 8 Acq On : 25 Feb 2002 5:01 pm Operator: • ’ Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Phenanthrene, 9-methyl- $$ ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 89300 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 45 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 45 Abundance Scan 1675 (22.283 min): 01142.D (-) m/z 192.00 100.00% 192

5000

96 82 ..................... ............................ . 22.00 22.20 22.40 22.60 0 111IIWPIPTTPTTT 70 rr I'1' i' । .... ll— m/Z 96.00 18.93% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 19/2

5000 22.00 22.20 22.40 22.60 m/z 191.00 17.52% ................... 88 20........... 139 152 165 176 U 0 ’1 | "TETR" । 11 [ । । > 11 > 11 । ■ । । ■ 111 111 i n ■ 11 । । 111 ।: । । 11 ■ 11 ■ 11 >| 111 । 1111 i । .I. < । > > 111 ‘111 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 193.10 16.89%

54 110

m&-> 30 0 ""I.... . " i " " i " " i 94 " । > 11111 ■1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 '' i " " I " " I " " I' " ' I" " I ‘" I ■'111 4 Abundance #103920: Anthracene, 9-methyl- 192 22.00 22.20 22.40 22.60 m/z 146.10 15.64%

5000

96 152 165 176 , Tuugt ............... . 0 i' ‘ ' r ■ " i " '' i " '' i " " i ■1 . ........................ . ..................... | > u 11.. m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

01142.D HP022102.M Tue Feb 26 08:30:35 2002 Page 13

NYC-WTC_000003539

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NYC-WTC_000003539Source: NYC Law Department, mirrored locally

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