GCMS analysis results for sample AE01142, Feb 2002

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Laboratory report documenting GCMS analysis of sample AE01142 conducted on February 27, 2002.

NYC-WTC_000003523–000003542

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01142.D Vial: 8 Acq On : 25 Feb 2002 5:01 pm Operator: •’ Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 10 Hydroxylamine, O-decyl- $$ ... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

13.41 0.08 ug/L 50520 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydroxylamine, O-decyl- $$ 0-Dec... 173 C10H23NO 029812-79-1 59 2 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 59 3 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 59 4 Undecane (CAS) $$ n-Undecane $$ ... 156 C11H24 001120-21-4 59 Abundance Scan 889 (13.410 min): 01142.D (-) m/z 57.10 100.00% 43 57

71 5000 /.......... 85 140

13.00 13.20 13.40 13.60 13.80 0 i * ■" I' " i1"' i1' 11011111101111111/1111117-011——3T0030333T m/ Z 43.10 97.79% z—> Abundance 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 #77514: Hydroxylamine, O-decyl- $$ O-Decylhydroxylamine . fl 43 57

5000 71 M AI1'1'I‘' 13.00 13.20 13.40 13.60 13.80 85 m/z 71.10 61.74%

0 a THT Tp-r- I i. 97 112 141 173 fl /z—> 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #154907: Hexadecane (CAS) $$ n-Hexadecane $$ Cetane $$ n-C... 43 57 ' ' I ' ' 1 ■ > । । । ■ 13.00 13.20 13.40 13.60 13.80 71 m/ Z 41.10 47.91% 5000 85

| 99 113 127 141 155 169 182 226 0 i11" i " ■ r1 — r i1"" i " '11" " i"'1 r ■''' r " ■ I'" " i1r ■ "T "' l1"' i" ■' i" " r " ■ r'1' i" m/z—> 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #113295: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane TTT 1 1 1 1 43 57 13.00 13.20 13.40 13.60 13.80 m/z 85.10 38.56%

5000 71 85

99 113 127 141 155 168 198 0 i" " i 1" i" 11" " r1 ■11 ■ I" । ■ TI1—1—a—ampuHmo TTT ■ i ■ ' 1 ■ । 1 ■ m/z-> ;30 40 50 60 70 80 90 100110120130140150160170180190200210220230 13.00 13.20 13.40 13.60 13.80

01142.D HP022102.M Tue Feb 26 08:30:35 2002 Page 12

NYC-WTC_000003538

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