GCMS analysis results for sample AE00106, Feb 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00106 analyzed on February 7, 2002.

NYC-WTC_000050774–000050792

Folder label: “GCMS X 1/4/02 A 1/25/02”

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN25\00106.D Vial: 5 Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 11 Phenanthrene, 9-methyl- $$ ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 114694 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 2 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 3 1,4-Dimethyl-3,5-propanobicyclo[... 192 C13H20O 000000-00-0 47 41H-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 000000-00-0 42 Abundance Scan 1656 (22.280 min): 00106.D (-) m/z 192.10 100.00% 192

5000 \ TTT 146 82 96 160 22.00 22.20 22.40 22.60

n/z-> 44 52 - ■ " ■ 1 ■'!' ■ l1 ■ 70 mmmpmn 120 '"I" "I........ . T’’ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 — JU m/z 191.10 17.24% Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

5000 TTT 22.00 22.20 22.40 22.60 m/z 193.10 16.07% 96 165 88 ,,| 139 152 ■ ■ ।" i " " r " • i ■ ’ " i ■ " ■ i ■11 • i" " r ” • i ■ ■" i " ■ ■ r " ■ i " " i ‘ ‘ | 176 , I... n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin.. 159 192

22.00 22.20 22.40 22.60 5000 m/z 146.10 15.45%

144 177

m/z-> 'I" । ।■ r ■" i i ■ ■ " i ■ " ' i " '' r " ' I 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 X — I''' * I Ir Abundance #103601:1,4-Dimethyl-3,5-propanobicyclo[2.2.2]octan-2-one / e T 107 192 22.00 22.20 22.40 22.60 159 m/z96.10 14.92% 119 93 5000 132 145 174

rn/z--> 40 50 ।"' ■ । i • ■ ■ ■ ।" i' " ■ r " ■ r ■ " i" ’ ’ i" " i 60 70 80 T ।" " । 90 100 110 120 130 140 150 160 170 180 190 200 U 22.00 22.20 22.40 22.60

30106.D SCAN508.M Mon Jan 28 09:49:54 2002 Page 13

NYC-WTC_000050790

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NYC-WTC_000050790Source: NYC Law Department, mirrored locally

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