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GCMS analysis results for sample AE00615, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00615 conducted on February 1, 2002.

NYC-WTC_000051624–000051641

Folder label: “GCMS X 1/9/02 A 1/29/02”

←Page 14 of 18→
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00615.D Vial: 4 ' Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *********************************************************** ** **** * * * * Peak Number 8 Cyclopentasiloxane, decamet... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.14 ug/L 91245 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 42 3 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 37 4 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 25 Abundance Scan 803 (12.541 min): 00615.D (-) m/ z 73.10 100.00% 73

5000 267 355 ' 1* 1 1 i' . \ pprvie . > . । । 45 12.20 12.40 12.60 12.80 191 ,i TTTTTTTTLTUTUTTTTTTTTTTDTITITIWUTITTTUTTTTTT m/z 267.00 42.79% n/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 — I ' 5000 1 1 1 1 1 1 1 1 1 ' 12.20 12.40 12.60 12.80 m/Z 355.10 39.21% 207 323 , ' I''' 'i'' " I " 1 'T1" 11111111111 " UTTITII n 11111111. A 111 " r " t " 'I'""I"'"i" " I" " r■'' i"" i1" mlz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 1 1 i ■ ' ■ 1 i ‘ ‘‘ 'I । । 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 13.60% 355 45

m/z-> +H 193 223 , TI] ■ • r '"I""i'I'""i" "i" " i" " i 323 l 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #357156: Noradrenaline tetraTMS 73 12.20 12.40 12.60 12.80 m/ z 74.00 7.96%

5000 102 355

45 ri" "i”" i 147 TOWTgT 442 ■ ■ i ■ ■ ■ ■ i ' T V m/z—> 40 60 80 100120140160180200220240260280 300320340 360 380400420440 12.20 12.40 12.60 12.80

30615.D SCAN508.M Wed Jan 30 09:02:21 2002 Page 10

NYC-WTC_000051637

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NYC-WTC_000051637Source: NYC Law Department, mirrored locally

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