GCMS analysis results for sample AE00615, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00615 conducted on February 1, 2002.

NYC-WTC_000051624–000051641

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN29\00615.D Vial: 4 Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 1-Cyanocarbazole $$ 9H-Carb... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 128677 Phenanthrene -dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 083415-88-7 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole ... 192 C13H8N2 057955-18-7 64 3 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 59 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 Abundance Scan 1656 (22.280 min): 00615.D (-) m/z 192.10 100.00% 192

5000 ........................... .........................

82 96 146 160 , 22.00 22.20 22.40 22.60

m/z-> 44 52 70 TTnuuum’u"nrr ■ ■ i ■ ■ ■ ■ i1 ■ ■ ■ i ■ ■111' "tf ‘337 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 al m/z 193.10 15.69% Abundance #103423:1-Cyanocarbazole $$ 9H-Carbazole-1 -carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 m/z 146.10 15.21% 164 96

nlz-> 40 "’ItT’’11-171"T"IE1TTT"ET’ITCIO’V"TTT । 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 । 138 ■ 11 ■ ■ < ■ । X ____ 1 i' ■ ■' i1

Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 A L 22.00 22.20 22.40 22.60 5000 m/ z 96.10 14.12%

96 164 , ' i " '11 ” ” i '■ A ................ .. ................. |l................. I I I . ′′′ | . . . i | . . . f] . . |T-|-FI I I I 17171 I I I I ITT’ I I |T I ‘' I'1 m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 22.00 22.20 22.40 22.60 m/z 191.10 13.13%

5000

96 164 1 138 lapaoan/l TTTTTTTTTTTTTTTTTTTTTTTT ' i ■ ■'' i ■ 11111 /z- > 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

)0615.D SCAN508.M Wed Jan 30 09:02:21 2002 Page 11

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