GCMS blank analysis results, Feb 25-26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\0116B.D Vial: 1 . Acq On : 25 Feb 2002 11:14 am Operator: Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Methyl-d3-hydrazine sulfate Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 9.44 0.04 ug/L 11734 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Methyl-d3-hydrazine sulfate 49 CH3D3N2 000000-00-0 3 2 1-Propenyl ester of carbonic acid 102 C4H603 000000-00-0 2 3 Propane, l-chloro-2-methyl- (CAS... 92 C4H9C1 000513-36-0 2 4 Propane, l-chloro-2-methyl- (CAS... 92 C4H9C1 000513-36-0 2 Abundance Scan 537 (9.436 min): 0116B.D (-) m/z 43.10 100.00% 43 57

49 5000

84 9.00 9.20 9.40 9.60 9.80 ‘ 0—T • i • • • • i » • • ■ । 1 ' I ■ • 1 • i ‘ ‘ ■ i ' m/z 57.00 82.28% mz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #281: Methyl-d3-hydrazine sulfate 49

5000 9.00 0 9.20 9.40 9.60 9.80 m/z 48.90 59.11%

m/z-> Abundance

5000 0-m" 1 1 1 ' i 1 1 1 1 i 1 1 > ' r — 10

15 20 30

29 40 50 l 1 ■

O) ■ ■ i • ■ ■ ■ i ■ 1 ' ■ i ■ ' ‘ ■ i 1 ■ • ' i ■ • • • i

70 80 #9103:1 -Propenyl ester of carbonic acid 43 lll 57 90 100 110

. L 9.00 m/z 9.20 44.00 9.40 9.60 9.80 52.37%

102 O’. • ( । । 1 i ■ ■ ■ ‘ i ' ■ ■ ■ i ■ ■ ■ 1 i ■ • ■ ■ i 1 1 ■ ■ i 1 • ■ ■ i miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance i#5490: Propane, 1-chloro-2-methyl- (CAS) $$ isobutyl chlor... । ■ * • * । > * 43 9.00 9.20 9.40 9.60 9.80 m/z 83.95 6.75% 5000

27

0 1 ' i ' ■ ■ ■ i ■ ■ ■ ■ i ■ • 37 ■ I , 49 56 63 1 ■ ‘ I ■ ■ ' ■ i 77 ' i ■ ' * ‘ ‘i 92 1

n/z—> 10 20 30 40 50 60 70 80 90 100 110 9.00 9.20 9.40 9.60 9.80

0116B.D HP022102.M Tue Feb 26 08:30:42 2002 Page 11

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