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← Document results/DEP Box 12/GCMS X 1/20/02 A 2/25/02
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GCMS blank analysis results, Feb 25-26 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.

NYC-WTC_000003425–000003443

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\0116B.D Vial: 1 Acq On : 25 Feb 2002 11:14 am Operator: Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.13 ug/L 60901 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 38 3 Pentasiloxane, 1,1,3,3,5,5,7,7,9... 356 C10H32O4Si5 000995-83-5 36 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 33 Abundance Scan 812 (12.540 min): 0116B.D (-) m/ z 73.00 100.00% 73

5000' 267 355 ' • i ■ • • ■ i ■ • ■ ■ i 1 1 1 1 i 1 1 1 ' I 12.20 12.40 12.60 12.80

n/z-> 0- a‘1‘11‘1‘001110"B—3B13TT‘T‘01111*131 193 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 211. n r n H m/z 267.00 44.39%

Abundance #313068: Cyclopentasiloxane, decamethyl- 73 355 267 / 5000 i 1 ■ ■ ■ i ■ i ■ ■ ■ ■ i 12.20 12.40 12.60 12.80 m/z 355.00 35.43% 323339 umgTTmm 191207 251 1 O-me ,I'1—mmmpautamo— n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 T i 1 ■ ■ T I • * ■ > I 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 13.75% 355 45 1 193 223 251 i niz-> 01 U 323339 । * j । » k ‘ p I » • ( । « » » j » » i i | ‘ • * » j » J f J | i 'l J I | ’l J l »’ | I ’Pr TTPr TPWTTTTTTTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #302654: Pentasiloxane, 1,1,3,3,5,5,7,7,9,9-decamethyl- • • । • i • --- 73 267 12.20 12.40 12.60 12.80 m/z 267.90 11.20% 133 5000 341 207 212 0 < । • 11 < > 11 > j ■ > < > I > । > 11 > > HHr 1111111 > । r . 211 326 1 356 ’ ’’I’ • ■ • i ■ ' ‘ i ■ । ■ 11 • 1111 ■ 11 ’*’14 mtz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80 TUT

0116B.D HP022102.M Tue Feb 26 08:30:42 2002 Page 12

NYC-WTC_000003439

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NYC-WTC_000003439Source: NYC Law Department, mirrored locally

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