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GCMS reference results for sample AE03454, Mar 13 2002

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Laboratory report listing quantitative results for various organic compounds in sample AE03454 from March 13, 2002.

NYC-WTC_000038391–000038398

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\022802\0226LB.D Vial: 6 Acq On : 28 Feb 2002 3:05 pm Operator: McLean * Sample : GC MS SCAN 2/27 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.79 ug/L 565427 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 58 3 Benzoic acid, 2-[ (trimethylsilyl... 282 C13H2203Si2 003789-85-3 47 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 993 (12.083 min): 022SLB.D (-) m/z 73.10 100.00% 73

5000 267 355 ■V | | . ' i if r

45 11.80 12.00 12.20 12.40 0- - TT i • '• 133 154—22233— 323 —t T m/z 267.00 44.41% m/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 -PP 11-80 12.00 12.20 12.40 355 m/z 355.10 37.13% 45 0- 26—14 96 133 165 193 • ' i' ' • -TPIr 293 323—4 m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 T-r-p-n-r-j-r r> i । i . i TIT 355 11.8012.0012.20 12.40 267 m/z 356.10 14.34% 5000

01 45 TIt — 201— ■250t 323 1 ; nfe-> 50 100 150 200 300 350 Abundance #227687: Benzoic acid, 2-[(trimethylsilyl)oxy], trimethyl... . . । . I M | 1 . | . i . | k 1 73 267 11.80 12.00 12.20 12.40 m/z 268.00 12.27%

5000

135 193

miz—> 0 47 IT 50 92.115.144124233 100 150 200 — 11 250 300 350 11.80 12.00 12.20 12.40

3226LB.D 5080202.M Wed Mar 13 06:41:06 2002 Page 3

NYC-WTC_000038397

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