GCMS analysis results for sample AE01002, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\022802\01002FB.D Vial: 15 Acq On : 28 Feb 2002 10:26 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.74 ug/L 488359 Naphthalene-d8 13.05

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-691 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 47 4 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 43 Abundance “ Scan 993 (12.083 min): 01002FB.D (-) m/ z 73.10 100.00% 73

5000 267 355 ' 1 1 I 1 ■ 1 1 i .+ I mmPrrrr j 45 11.80 12.00 12.20 12.40 j 223 „ 0 — 1* 125 *** 154 1*14 193 Arpran — — IPT 323 ' 1 1 1 1 1 1 1 I ' 1 m/z 267.00 43.11% m/z->_ Abundance 50 100 150 200 250 300 350 400 450 #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 T-rp-r-r-r-pH- ' i ' ' ' ' i ' ■ 11.80 12.00 12.20 12.40 ! 355 m/z 355.10 39.75% 45 0 ] : | 103 133,165 193 223.4 293 323 1....................... m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

TPIUTTTT 355 11.80 12.00 12.20 12.40 | 267 m/z 356.00 12.77% 5000- i

45 0 / 207 i 4 - 323 T-r-p-r-r-r-p-r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73 11.80 12.00 12.20 12.40 I m/z 268.00 11.13%

5000 355

147 47 105 193 237 267295 325 384 429457 0 T-r-j-W ‘ t T m/z-> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

01002FB.D 5080202.M Wed Mar 13 10:57:22 2002 Page 3

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