GCMS analysis results for sample AE01047, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\022802\01047FB.D Vial: 16 Acq On : 28 Feb 2002 11:15 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.29 ug/L 377849 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 43 4 N- (Trifluoroacetyl)-N,0,0‘,0‘‘-t... 553 C22H42F3N04Si4 000000-00-0 43 Abundance Scan 993 (12.083 min): 01047FB.D (-) m/z 73.10 100.00% 73

5000 267 355

45 11.80 12.00 12.20 12.40 01 I I 133154 193 223 ,| 323,3504— m/z 267.00 45.64% ' i r TITTTI m/z-> 50 100 150 200 250 300 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 ■ ■ ■ । > ■ ■ > । • i • ■ ‘ • i ■ ► ‘ > 11.80 12.00 12.20 12.40 355 m/z 355.10 39.06% 45 0 — 96 133 165 193, 223 247 293 323 — m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 11.80 12.00 12.20 12.40 267 m/z 356.10 13.17% 5000

45 0 207 323 , 1——Im rn/z-> 50 100 150 200 250 300 350 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... ■ ■ ■ i ■ ' ' ■ i ■ ■ ■ 1 I 1 ' ' 1 i1' 1 1 73 11.80 12.00 12.20 12.40 m/z 268.00 11.65%

5000 355

44

267 294 0- #+—4 93 116 147 193 220 , 384 m/z-> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40

11047FB.D 5080202.M Wed Mar 13 11:03:31 2002 Page 3

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